Synthesis and anticorrosion studies of 4-[(2-nitroacetophenonylidene)-amino]-antipyrine on SAE 1012 carbon steel in 15 wt.% HCl solution

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dc.authorid0000-0002-9663-4264en_US
dc.authorid0000-0003-0401-7419en_US
dc.authorid0000-0002-5208-355Xen_US
dc.authorid0000-0002-3251-8846en_US
dc.authorid0000-0003-1579-6411en_US
dc.contributor.authorGerengi, Hüsnü
dc.contributor.authorÇakmak, Reşit
dc.contributor.authorDağ, Beşir
dc.contributor.authorSolomon, M. M
dc.contributor.authorTüysüz Akbal, Hatice Aslıhan
dc.contributor.authorKaya, Ertuğrul
dc.date.accessioned2021-04-13T05:54:54Z
dc.date.available2021-04-13T05:54:54Z
dc.date.issued2020-11-16en_US
dc.departmentBatman Üniversitesi Fen - Edebiyat Fakültesi Kimya Bölümüen_US
dc.departmentBatman Üniversitesi Sağlık Hizmetleri Meslek Yüksekokulu Tıbbi Hizmetler ve Teknikler Bölümüen_US
dc.description.abstractA novel corrosion inhibitor, ((E)-1,5-dimethyl-4-((1-(3-nitrophenyl)ethylidene)amino)-2-phenyl-1,2-dihydro-3H-pyrazol-3-one) (DNPP) was synthesized in high yield by the condensation reaction of 4-aminoantipyrine with 2-nitroacetphenone derived from acetophenone as a starting material and characterized by FT-IR, 1H, and 13C NMR techniques. DNPP was tested against the corrosion of SAE 1012 carbon steel in 15 wt.% HCl solution using electrochemical and surface characterization techniques. Results obtained show that DNPP is effective in retarding the corrosion of SAE 1012 carbon steel. With 4 mM of DNPP, the charge transfer resistance of SAE 1012 in 15 wt.% HCl solution is raised from 17.42 to 140.50 Ω cm2 and the substrate surface is protected by 87%. The inhibition is through adsorption mechanism (mixed-adsorption type) and has been confirmed by SEM and EDAX results. Potentiodynamic polarization results reveal that DNPP acted as a mixed-type corrosion inhibitor. DNPP is a promising candidate for the formulation of an inhibitor cocktail for the strong acid environment.en_US
dc.identifier.citationGerengi, H., Çakmak, R., Dağ, B., Solomon, M. M., Tüysüz Akbal, H. A., Kaya, E. (2020). Synthesis and anticorrosion studies of 4-[(2-nitroacetophenonylidene)-amino]-antipyrine on SAE 1012 carbon steel in 15 wt.% HCl solution. Journal of Adhesion Science and Technology, 34 (22), pp. 2448-2466. https://doi.org/10.1080/01694243.2020.1766400en_US
dc.identifier.endpage2466en_US
dc.identifier.issn0169-4243
dc.identifier.issn1568-5616
dc.identifier.issue22en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage2448en_US
dc.identifier.urihttps://doi.org/10.1080/01694243.2020.1766400
dc.identifier.urihttps://www.tandfonline.com/doi/pdf/10.1080/01694243.2020.1766400?needAccess=true
dc.identifier.urihttps://hdl.handle.net/20.500.12402/2848
dc.identifier.volume34en_US
dc.identifier.wosqualityQ3en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherTaylor & Francisen_US
dc.relation.isversionof10.1080/01694243.2020.1766400en_US
dc.relation.journalJournal of Adhesion Science and Technologyen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/embargoedAccessen_US
dc.rightsAttribution-NonCommercial-ShareAlike 3.0 United States*
dc.rights.urihttp://creativecommons.org/licenses/by-nc-sa/3.0/us/*
dc.subject4-Aminoantipyrineen_US
dc.subjectSchiff Baseen_US
dc.subjectCarbon Steelen_US
dc.subjectCorrosionen_US
dc.subjectCorrosion Inhibitionen_US
dc.titleSynthesis and anticorrosion studies of 4-[(2-nitroacetophenonylidene)-amino]-antipyrine on SAE 1012 carbon steel in 15 wt.% HCl solutionen_US
dc.typeArticleen_US

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