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Öğe Hydrothermal synthesis of magnetic nanocomposite from biowaste matrix by a green and one-step route: Characterization and pollutant removal ability(Elsevier, 2019-04) Sayğılı, HasanThis study aimed to produce an industrial waste-based novel magnetic nanocomposite (Fe@GPHC) by a facile and one-step hydrothermal carbonization (HTC) method. In order to characterize of Fe@GPHC, X-ray fluorescence spectroscopy (XRF), Scanning electron microscopy-energy dispersive X-ray spectroscopy (SEM-EDX), X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FT-IR), Brunauer-Emmett-Teller (BET), Vibrating-sample magnetometer (VSM), and elemental (ultimate) analyses were applied. Characterization results showed that during the HTC process, the Fe nanoparticles (FeNPs) were successfully incorporated on biowaste matrix. In addition, the Fe@GPHC was used to test its adsorptive property. For this, methylene blue (MB) and methyl orange (MO) were selected as a simulated pollutant. A batch method was used to perform the adsorption experiments. The maximum adsorption capacity of Fe@GPHC was 11 mg g(-1) and 8.9 mg g(-1) for MB and MO, respectively. This study provides a feasible and simple approach to design and synthesis of high-performance functional magnetic material in a cost-effective way.Öğe Optimized preparation for bimodal porous carbon from lentil processing waste by microwave-assisted K 2 CO 3 activation: Spectroscopic characterization and dye decolorization activity(Elsevier, 2019) Sayğılı, Hasan; Akkaya Sayğılı, GülbaharThis paper describes lab-scale experiments for producing optimal activated carbon (LWAC)with bimodal porous (mixed micro-mesoporous)texture under optimized conditions from lentil processing waste (LW)by microwave-assisted K 2 CO 3 activation. The influences of various operating parameters were evaluated including impregnation ratio (IR), carbonization temperature (CT)and carbonization time (Ct). The BET surface area (S BET )and total pore volume (V T )were chosen as main criteria in optimization. The optimized parameters were IR ratio of 3:1, CT of 800 °C and Ct of 1 h. The physicochemical properties of LW and LWAC were identified with diverse analytical techniques. LWAC possessed high S BET of 1875 m 2 /g and large V T of 0.995 cm 3 /g. The LWAC was then tested for its feasibility as cationic (Methylene blue (MB))and anionic (Methyl orange (MO))dyes adsorbent. It was found that LWAC has an adsorption capacity of 625 mg/g for MB and 476 mg/g for MO at 30 °C
