Synthesis, characterization and experimental, theoretical, electrochemical, antioxidant and antibacterial study of a new Schiff base and its complexes

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dc.authorid0000-0001-5792-419Xen_US
dc.contributor.authorBaykara, Hacı
dc.contributor.authorİlhan, Salih
dc.contributor.authorLevent, Abdulkadir
dc.contributor.authorSeyitoğlu, Mehmet Salih
dc.contributor.authorÖzdemir, Sadin
dc.contributor.authorOkumuş, Veysi
dc.contributor.authorÖztomsuk, Abdussamet
dc.contributor.authorCornejo, Mauricio
dc.date.accessioned2021-03-23T07:01:44Z
dc.date.available2021-03-23T07:01:44Z
dc.date.issued2014-09-15en_US
dc.departmentBatman Üniversitesi Fen - Edebiyat Fakültesi Kimya Bölümüen_US
dc.description.abstractA new Schiff base ligand was synthesized by reaction of salicylaldehyde with 1,6-bis(4-chloro-2-aminophenoxy)hexane. Then the Schiff base complexes were synthesized by metal salts and the Schiff base. The metal to ligand ratio of metal complexes was found to be 1:1. The Cu(II) complex is proposed to be square planar and the Co(II), Ni(II), Mn(II) and Zn(II) complexes are proposed to be tetrahedral geometry. The Ti(III) and V(III) complexes are proposed to be a capped octahedron in which a seventh ligand has been added to triangular face. The complexes are non-electrolytes as shown by their molar conductivities (ΛM). The structure of metal complexes is proposed from elemental analysis, FT-IR, UV–vis, magnetic susceptibility measurements, molar conductivity measurements, Mass Spectra and thermal gravimetric analysis. In addition antimicrobial and antioxidant studies, cyclic voltammetry of the complexes, theoretical 1H NMR and HOMO–LUMO energy calculations of the new di-functional ligand were done.en_US
dc.identifier.citationBaykara, H., İlhan, S., Levent, A., Seyitoğlu, M. S., Özdemir, S., Okumuş, V., Öztomsuk, A., Cornejo, M. (2014). Synthesis, characterization and experimental, theoretical, electrochemical, antioxidant and antibacterial study of a new Schiff base and its complexes. Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 130, pp. 270-279. https://doi.org/10.1016/j.saa.2014.03.094en_US
dc.identifier.endpage279en_US
dc.identifier.issn1386-1425
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage270en_US
dc.identifier.urihttps://doi.org/10.1016/j.saa.2014.03.094
dc.identifier.urihttps://hdl.handle.net/20.500.12402/2760
dc.identifier.volume130en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherElsevieren_US
dc.relation.isversionof10.1016/j.saa.2014.03.094en_US
dc.relation.journalSpectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopyen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/embargoedAccess*
dc.rightsAttribution-NonCommercial-ShareAlike 3.0 United States*
dc.rights.urihttp://creativecommons.org/licenses/by-nc-sa/3.0/us/*
dc.subject1,6-Bis (4-chloro-2-aminophenoxy) Hexaneen_US
dc.subjectCyclic Voltammetryen_US
dc.subjectSalicyaldehydeen_US
dc.subjectBiological Activitiesen_US
dc.subjectMass Spectraen_US
dc.subjectGaussian 09 and HOMO–LUMOen_US
dc.titleSynthesis, characterization and experimental, theoretical, electrochemical, antioxidant and antibacterial study of a new Schiff base and its complexesen_US
dc.typeArticleen_US

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